Surface Area & Pore Size

Surface Area & Pore Size Analyzer

SA-2000PS Series

More info

P0 test: an independent vapor pressure (P0) test stations, to ensure high accuracy of the partial pressure of the test;
Sample preparation: number of samples processed simultaneously: 2/2/4 pcs; two-way degassing station has an independent temperature control, and an independent timing, at different temperatures and at different times of the sample degassing treatment can support and test carried out simultaneously;
Sample preparation mode: having the domestic unique "conventional heating vacuum molecular diffusion mode" and "molecular replacement mode" in two optional features; molecular replacement mode molecular diffusion model efficiency by more than 1 times, can save more than half of the pre-treatment time to solve the conventional sample preparation method static problem a long time;
Stress Test: Stress Test Range 0-1.6bar (0-160KPa), accuracy error ≤0.15%;
Liquid nitrogen level control: a liquid nitrogen holding surface servo system, the elimination of the testing process because the liquid nitrogen so that nitrogen volatilization surface changes brought dead volume change, improve test accuracy;
Atmospheric recovery: a leading domestic and international testing, degassing is completed automatically restore normal pressure function for easy removal, anti-splash sample;
Intelligent self-checking system: The instrument has a self-test hardware and pneumatic tightness self-test function, can automatically detect the sample tube is installed, the jacket tubes are tightened, and check to make sure the location of the leak, given text prompts and voice prompts;
Voice prompts: a unique intelligent real voice prompts;
Software interface:
   1, graphical control interface: pro and control and monitoring interface, complex instruments work in the form of a state diagram to show that the instrument work status at a glance, and the structure of the various valves, vacuum, nitrogen Cup lift All hardware, operating temperature, etc., pleasing;
  2, custom style conversion: style software interface can be converted to the user's preferences;
Control System:
   1, strong and stable control system to prevent accidents; instrument with real-time data storage function and status, in the long run the process automatically, even when the data line is disconnected, unexpected power outages and other unforeseen circumstances, it served as the instrument to restart and then can be restored test data into the test process continue testing;
   2, when the cup of liquid nitrogen at the top, if not decline in liquid nitrogen and vacuum cup, the temperature rises, the gas adsorption quickly overflow the sample tube, so that the risk of sample tube burst; SA-2000PS series instrument has a leading domestic intelligence and security liquid nitrogen Cup "safe drop" control systems to prevent accidents, the key point of the system is that the operator cannot be controlled at the liquid nitrogen cup drop, even when unexpected power failure or restart the device, the device automatically enters the liquid nitrogen Cup "security drop "process;
   3, at home and abroad leading pump start-stop management system, during the test has been running without a vacuum pump to reduce noise and prolong the life of the vacuum pump;
   4, the operation of the instruments detailed logging; the instrument run logs automatically record the results of each command and the instrument in the instrument during the operation, including the switching valve, pump start and stop, the original acquisition data, accurate to the second time. The log for the reliable operation of the instrument to provide protection and after-sale;

Data processing 
   1, isotherm analysis has a standard mode, fine mode and custom modes, aperture can be set request for key segments for fine analysis;
   2, custom testing process: test can be adsorbed, adsorption-desorption tests, and directly into the desorption test (automatic rapid adsorption saturation);
  3, a variety of options to test the theory, there is a chart graphs, histograms;
4, a powerful data management and processing system: the raw data and the calculation of all the test results are stored as SQL database support by date, operator and sample names, etc. Find filtering capabilities; support for bulk export;

Performance parameters


Product Comparison Name

Static volumetric method and BJH analyzer

Product name

SA-2000PS1 type
Surface area and pore size analyzer

SA-2000PS2 type
Surface area and pore size analyzer

SA-2000PS4 type
Surface area and pore size analyzer

Model

SA-2000PS1

SA-2000PS2

SA-2000PS4

Product Image

H78cm*W50cm*L47cm
Weight:32Kg

H78cm*W50cm*L47cm
Weight:36Kg

H78cm*W72cm*L47cm
Weight:46Kg

Function

Surface area, Microporous, pore size analysis

Testing method

Static volumetric method

analysis station number

2sample degassing station;
1 P0 test stations;
1sample analysis station;

2sample degassing station;
1 P0 test stations;
2sample analysis station;

4sample degassing station;
1 P0 test stations;
4sample analysis station;

Theory and test report

1, adsorption and desorption isotherms;
2, BET single point method;
3, BET multi-point method, BET constant C;
4, Langmuir (Langmuir) multi-point method; Langmuir equilibrium constant b;
5, the outer surface area statistical method adsorption layer thickness (STSA) S outside;
6, estimate and report the size and true density;
7, BJH pore volume of pore size distribution; (differential and integral pore volume, pore size, pore size distribution histograms, graphs)
8, MK-plate method (parallel plate model) pore volume, pore size distribution (to complement the BJH method, lamellar structure suitable for materials analysis)
9, t-plot method (Boder) microporous analysis; (V-t diagram, t law pore size distribution)
10, MP method (Brunauer) microporous analysis; (V-t diagram, pore size distribution) (which take into account the different adsorbed material constants different factors than the t-plot method close to the true value)
11, D-R Act (Dubinin- Astakhov) microporous analysis;
                                 

Test Accuracy

                               Repeatability error is less than ± 1.5%

Test Range

Specific surface area 0.01m2 / g or more, the microporous 0.35-2nm; mesoporous 2-50 nm; macropores to be 50-500nm; sample types: powders, granules, fibrous sheet material and the like can be loaded into sample tube material

Advantages and Disadvantages

Surface area and pore size for analysis, especially for the large specific surface area and porosity developed sample resolution, high accuracy, suitable catalysts, molecular sieves and other porous, large surface area of ​​the sample surface area and pore size distribution analysis test.

Pressure Measurement

Smart investment volume control, the small amount of adsorption sample 2-3min / dividing point, the large amount of adsorption sample 3-5min / dividing point;
BET multi-point method 15-30min / set of samples;
BET single point method 6-10min / set of samples;
Aperture standard test 60-120min / set of samples;
Narrow aperture test 120-300min / set of samples; (1, number of samples and the number of stations in each group simultaneously test instrument analysis related; 2, more testing time does not include sample preparation time;)

Ultimate vacuum

Mechanical pump, 4 × 10

Liquid nitrogen Cup

2L large volume liquid nitrogen Dewar Cup, kept growing up to 100h, 70h continuous testing without adding liquid nitrogen. Another optional 3L micro analysis Dewar Cup, when the insulation is greater than 140h, 90 hours no need adding liquid nitrogen

Sample pretreatment

Degassing
(Normal mode: heating, vacuum; molecular replacement mode: heating, vacuum, nitrogen injection cycle;)

Pretreatment time

Molecular replacement mode: 60-180min; Normal mode: 120-240min;

Power supply:

 AC 220v ± 10%, the current frequency of 50 Hz, power less than 200 watts

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